Nanoindentation study of the combined effects of crystallography, heat treatment and exposure to high-flux deuterium plasma in tungsten

TitleNanoindentation study of the combined effects of crystallography, heat treatment and exposure to high-flux deuterium plasma in tungsten
Publication TypeJournal Article
Year of Publication2017
AuthorsY. Zayachuk, D.EJ Armstrong, K. Bystrov, S. van Boxel, T. Morgan, S.G Roberts
JournalJournal of Nuclear Materials
Volume486
Pagination183-190
Date Published04/2017
Abstract

Tungsten samples were heat-treated to achieve partial recrystallization and exposed to high ion flux deuterium plasma at different temperatures and fluences. Continuous stiffness nanoindentation measurements of near-surface hardness were performed in the grains of specific annealing states and of specific crystallographic orientation, determined by electron backscatter diffraction (EBSD); indentation pile-up was investigated using surface profilometry. Bulk hardness of unexposed tungsten does not strongly depend on grain orientation, but depends on the annealing state of the grain, with values between ∼4.3 GPa for recrystallized grains and ∼5.5 for non-recrystallized ones. Grains with <111> surface normal orientation feature the least pile-up, while grains with <001> orientation the most; pile-up also depends on the annealing state, being generally lower in recrystallized grains. Plasma exposure leads to the increase of hardness, most significantly near the surface. The width of plasma-affected zone increases with the increase of exposure temperature and fluence, as well in recrystallized grains, correlating with the increase of diffusion depth. Plasma exposure does not lead to the emergence of orientation-dependence of hardness. Both indentation pile-up and near-surface indentation pop-ins are generally suppressed by plasma exposure.

URLhttp://www.euro-fusionscipub.org/wp-content/uploads/WPMATPR16_16605_submitted.pdf
DOI10.1016/j.jnucmat.2017.01.026
Division

FP

Department

PMI

PIDa95fb19406b8be9d710cae9731d7a93f
Alternate TitleJ. Nucl. Mater.
LabelOA

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